Data Collection |
|
Space group | P212121 |
Unit cell (a, b, c, Å) | 68.9, 87.8, 138.5 |
Resolution (Å) | 2.07 |
Unique reflections | 47,379 |
-Fold of redundancy | 12.9 |
Completeness (%) | 91.1 (48.2)a |
Average I/σ | 12.0 (3.6)a |
Rmerge | 0.051 (0.28)a |
Structure Refinement | |
R factor | 0.216 |
Rfree | 0.248 (10%)b |
Resolution (Å) | 30-2.07 |
Reflections | 45,502 |
RMS deviation for Bond (Å) | 0.006 |
Angle | 1.1° |
Average B-factor (Å2) | |
Protein | 43.4 (4720)c |
Vardenafil | 35.2 (68)c |
Waters | 40.3 (183)c |